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Fibers, Volume 8, Issue 9 (September 2020) – 8 articles

Cover Story (view full-size image): Current FRP composites lack ductility and fail abruptly. By integrating a combination of fiber orientations and stacking sequences using 3D printing technology, we propose a new method for producing next-generation FRP composites that demonstrate progressive pseudo-ductile failure. View this paper.
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11 pages, 2081 KiB  
Article
A Novel Method of Spectra Processing for Brillouin Optical Time Domain Reflectometry
by Fedor L. Barkov, Yuri A. Konstantinov and Anton I. Krivosheev
Fibers 2020, 8(9), 60; https://doi.org/10.3390/fib8090060 - 22 Sep 2020
Cited by 13 | Viewed by 2668
Abstract
A new method of Brillouin spectra post-processing, which could be applied in modern distributed optical sensors: Brillouin optical time domain analyzers/reflectometers (BOTDA/BOTDR), has been demonstrated. It operates by means of the correlation analysis performed with special technique («backward-correlation»). It does not need any [...] Read more.
A new method of Brillouin spectra post-processing, which could be applied in modern distributed optical sensors: Brillouin optical time domain analyzers/reflectometers (BOTDA/BOTDR), has been demonstrated. It operates by means of the correlation analysis performed with special technique («backward-correlation»). It does not need any additional data for time or space averaging and operates with the single spectrum only. We have simulated the method accuracy dependence on signal-to-noise ratio (SNR) and other parameters. It is shown that the new method produces better results at low SNRs than conventional technique, based on finding of Brillouin spectrum maximum, do. These results are in a good agreement with the experiment. Finally, we have estimated the performance of the new method for its application in polarization-BOTDA set-up for a polarization maintaining (PM) fiber modal birefringence distributed study. Full article
(This article belongs to the Special Issue Optical Fibers as a Key Element of Distributed Sensor Systems)
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17 pages, 3851 KiB  
Article
Determination of Optimum Twist Equation for the Long Staple Combed Cotton Ring-Spun Yarn
by Dunja Šajn Gorjanc and Neža Sukič
Fibers 2020, 8(9), 59; https://0-doi-org.brum.beds.ac.uk/10.3390/fib8090059 - 21 Sep 2020
Viewed by 5288
Abstract
The aim of this research was to determine the optimum twist equation for ring-spun yarns. The yarn twist can be calculated by different equations. With the research, we tried to find the appropriate equation to determine the yarn twist, which is determined by [...] Read more.
The aim of this research was to determine the optimum twist equation for ring-spun yarns. The yarn twist can be calculated by different equations. With the research, we tried to find the appropriate equation to determine the yarn twist, which is determined by the values of yarn strength and hairiness. In the research, yarns from long staple combed cotton rovings and of different fineness (10 tex, 11.8 tex, 20 tex and 29.4 tex) were analyzed. The yarn twist was calculated using the equations of Koechlin and Laetsch. The analyzed yarns were produced in the spinning mill on the laboratory ring spinning machine Spinntester. In the second part of the investigation, yarn strength and hairiness were analyzed as a function of yarn twist. The results showed that Laetsch’s equation is suitable for determining the twist for yarns with a fineness of 10 tex, 11.8 tex, 20 tex and 29.4 tex, since, in this case, the calculated number of yarn threads is higher and thus the strength and elongation at break are also higher. The yarn hairiness is higher in analyzed samples for yarns with the twist calculated according to the Koechlin’s equation. Full article
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11 pages, 4109 KiB  
Article
Influence of Gamma Radiation on Mechanical Properties of Jute Fabric-Reinforced Polymer Composites
by K.Z.M. Abdul Motaleb, Rimvydas Milašius and Abdul Ahad
Fibers 2020, 8(9), 58; https://0-doi-org.brum.beds.ac.uk/10.3390/fib8090058 - 13 Sep 2020
Cited by 20 | Viewed by 4317
Abstract
Woven jute fabric was used as a reinforcing material for making two types of composite, named Jute/PR and Jute/Epoxy, with two different matrixes of polyester resin and epoxy, respectively, by hand layup techniques. Five different doses of gamma radiation from 100 to 500 [...] Read more.
Woven jute fabric was used as a reinforcing material for making two types of composite, named Jute/PR and Jute/Epoxy, with two different matrixes of polyester resin and epoxy, respectively, by hand layup techniques. Five different doses of gamma radiation from 100 to 500 krad were used to investigate the effects of the mechanical properties of the composites and the jute fabrics. Though gamma radiation improved the mechanical properties, such as the tensile strength (TS) and Young’s modulus (Y), and decreased the elongation at break % (Eb%) of the composites, it deteriorated all these properties for jute fabrics. The highest values of TS and Y and the lowest value of Eb% were found to be 39.44 Mpa, 1218.33 Mpa, and 7.68% for the Jute/PR; and 48.83 Mpa, 1459.67 Mpa, and 3.68% for the Jute/Epoxy composites, respectively, at a 300 krad gamma radiation dose. A further increase in dose altered all these properties; thus, 300 krad was found to be the optimum dose for both of the composites. Between the two composites, gamma radiation influenced the Jute/PR composite more than the Jute/Epoxy composite. Full article
(This article belongs to the Special Issue Natural Fibers and Composites: Science and Applications)
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16 pages, 2658 KiB  
Article
Wettability and Anti-Corrosion Performances of Carbon Nanotube-Silane Composite Coatings
by Luigi Calabrese, Amani Khaskoussi and Edoardo Proverbio
Fibers 2020, 8(9), 57; https://0-doi-org.brum.beds.ac.uk/10.3390/fib8090057 - 10 Sep 2020
Cited by 22 | Viewed by 3195
Abstract
In this paper, a sol-gel N-propyl-trimethoxy-silane coating filled with different amount of multi-wall carbon nanotubes (MWCNTs) was investigated in order to improve the aluminum corrosion resistance. The nanocomposite coating was applied, by drop casting, on AA6061 aluminum alloy substrate. The morphological analysis highlighted [...] Read more.
In this paper, a sol-gel N-propyl-trimethoxy-silane coating filled with different amount of multi-wall carbon nanotubes (MWCNTs) was investigated in order to improve the aluminum corrosion resistance. The nanocomposite coating was applied, by drop casting, on AA6061 aluminum alloy substrate. The morphological analysis highlighted that a uniform sol-gel coating was obtained with 0.4 wt.% CNT. Lower or higher nanotube contents lead to the formation of heterogeneities or agglomeration in the coating, respectively. Furthermore, all nanocomposite coatings exhibited effective adhesion to the substrate. In particular, the pull-off strength ranged in 0.82–1.17 MPa. Corrosion protection of the aluminum alloy in NaCl 3.5 wt.% electrolyte (seawater) was significantly improved after CNT addition to the base coating. The stability in electrochemical impedance was observed during three days of immersion in the sodium chloride solution. AS3-CNT2 and AS3-CNT4 batches showed advanced electrochemical stability during immersion tests. Furthermore, interesting results were evidenced in potentiodynamic polarization curves where a decrease of the corrosion current of at least two order of magnitude was observed. Moreover, the breakdown potential was shifted toward noble values. Best results were observed on AS3-CNT6 specimen which exhibited a passivation current density of approximately 1.0 × 10−5 mA/cm2 and a breaking potential of 0.620 V/AgAgClsat. Full article
(This article belongs to the Special Issue Carbon Based Composites for Advanced Sustainable Technologies)
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13 pages, 1959 KiB  
Article
Meso-Scale Formulation of a Cracked-Hinge Model for Hybrid Fiber-Reinforced Cement Composites
by Enzo Martinelli, Marco Pepe and Fernando Fraternali
Fibers 2020, 8(9), 56; https://0-doi-org.brum.beds.ac.uk/10.3390/fib8090056 - 01 Sep 2020
Cited by 11 | Viewed by 3057
Abstract
This study presents a non-linear cracked-hinge model for the post-cracking response of fiber-reinforced cementitious composites loaded in bending. The proposed displacement-based model follows a meso-mechanical approach, which makes it possible to consider explicitly the random distribution and orientation of the reinforcing fibers. Moreover, [...] Read more.
This study presents a non-linear cracked-hinge model for the post-cracking response of fiber-reinforced cementitious composites loaded in bending. The proposed displacement-based model follows a meso-mechanical approach, which makes it possible to consider explicitly the random distribution and orientation of the reinforcing fibers. Moreover, the model allows for considering two different fiber typologies whereas the cement matrix is modelled as a homogeneous material. The proposed mechanical model combines a fracture-based, stress-crack opening relationship for the cementitious matrix with generalized laws aimed to capture the crack-bridging effect played by the reinforcing fibers. These laws are derived by considering both the fiber-to-matrix bond mechanism and fiber anchoring action possibly due to hooked ends. The paper includes a numerical implementation of the proposed theory, which is validated against experimental results dealing with fiber-reinforced cement composites reinforced with different short fibers. The excellent theory vs. experiment matching demonstrates the high technical potential of the presented model, obtained at a reasonable computational cost. Full article
(This article belongs to the Special Issue Mechanics of Fiber Reinforced Cementitious Composites)
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10 pages, 5633 KiB  
Article
Stabilization and Incipient Carbonization of Electrospun Polyacrylonitrile Nanofibers Fixated on Aluminum Substrates
by Jan Lukas Storck, Timo Grothe, Khorolsuren Tuvshinbayar, Elise Diestelhorst, Daria Wehlage, Bennet Brockhagen, Martin Wortmann, Natalie Frese and Andrea Ehrmann
Fibers 2020, 8(9), 55; https://0-doi-org.brum.beds.ac.uk/10.3390/fib8090055 - 21 Aug 2020
Cited by 11 | Viewed by 3318
Abstract
Polyacrylonitrile (PAN) nanofibers, prepared by electrospinning, are often used as a precursor for carbon nanofibers. The thermal carbonization process necessitates a preceding oxidative stabilization, which is usually performed thermally, i.e., by carefully heating the electrospun nanofibers in an oven. One of the typical [...] Read more.
Polyacrylonitrile (PAN) nanofibers, prepared by electrospinning, are often used as a precursor for carbon nanofibers. The thermal carbonization process necessitates a preceding oxidative stabilization, which is usually performed thermally, i.e., by carefully heating the electrospun nanofibers in an oven. One of the typical problems occurring during this process is a strong deformation of the fiber morphologies—the fibers become thicker and shorter, and show partly undesired conglutinations. This problem can be solved by stretching the nanofiber mat during thermal treatment, which, on the other hand, can lead to breakage of the nanofiber mat. In a previous study, we have shown that the electrospinning of PAN on aluminum foils and the subsequent stabilization of this substrate is a simple method for retaining the fiber morphology without breaking the nanofiber mat. Here, we report on the impact of different aluminum foils on the physical and chemical properties of stabilized PAN nanofibers mats, and on the following incipient carbonization process at a temperature of max. 600 °C, i.e., below the melting temperature of aluminum. Full article
(This article belongs to the Special Issue Carbon Based Composites for Advanced Sustainable Technologies)
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13 pages, 6873 KiB  
Article
Modeling the Influence of Knots on Douglas-Fir Veneer Fiber Orientation
by Rémy Frayssinhes, Stéphane Girardon, Louis Denaud and Robert Collet
Fibers 2020, 8(9), 54; https://0-doi-org.brum.beds.ac.uk/10.3390/fib8090054 - 21 Aug 2020
Cited by 4 | Viewed by 2532
Abstract
This study presents a method for predicting the local fiber orientation of veneers made from peeled Douglas-fir logs based on the knowledge of the tree branch characteristics (location, radius, insertion angle, azimuth angle, and living branch ratio). This model is based on the [...] Read more.
This study presents a method for predicting the local fiber orientation of veneers made from peeled Douglas-fir logs based on the knowledge of the tree branch characteristics (location, radius, insertion angle, azimuth angle, and living branch ratio). This model is based on the Rankine oval theory approach and focuses on the local deviation of the fiber orientation in the vicinity of knots. The local fiber orientation was measured online during the peeling process with an in-house-developed scanner based on the tracheid effect. Two logs from the same tree were peeled, and their ribbons were scanned. The knot locations and fiber orientation were deduced from the scanner data. The first objective was to compare the fiber orientation model with measurements to enhance and validate the model for French Douglas-fir. The second objective was to link data measurable on logs to veneer quality. Full article
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20 pages, 6179 KiB  
Article
3D-Printed Pseudo Ductile Fiber-Reinforced Polymer (FRP) Composite Using Discrete Fiber Orientations
by Shreya Vemuganti, Eslam Soliman and Mahmoud Reda Taha
Fibers 2020, 8(9), 53; https://0-doi-org.brum.beds.ac.uk/10.3390/fib8090053 - 20 Aug 2020
Cited by 12 | Viewed by 4637
Abstract
The use of fiber-reinforced polymer (FRP) composite materials are continuously growing in civil infrastructure due to their high strength, low weight, and manufacturing flexibility. However, FRP is characterized by sudden failure and lacks ductility. When used in construction, gradual failure of FRP components [...] Read more.
The use of fiber-reinforced polymer (FRP) composite materials are continuously growing in civil infrastructure due to their high strength, low weight, and manufacturing flexibility. However, FRP is characterized by sudden failure and lacks ductility. When used in construction, gradual failure of FRP components is desired to avoid catastrophic structural collapse. Due to its mechanical orthotropy, the behavior of FRP relies significantly on fiber orientation and stacking sequence. In this paper, a novel multi-angled glass fiber reinforced polymer (GFRP) composite laminate showing pseudo ductile behavior is produced using 3D-printing. This is accomplished by varying fiber orientation angles, stacking sequence, and thickness of lamina. Single-angled GFRP composite specimens were 3D-printed with different fiber orientation angles of 0°, 12°, 24°, 30°, 45°, and 90° using continuous and fused filament techniques. The tension test results of the single-angled specimens were then used to aid the design of multi-angled laminate for potential progressive failure behavior. A 3D finite element (FE) model was developed to predict the response of the experimental results and to provide insight into the failure mechanism of the multi-angled laminate. The experimental observations and the FE simulations show the possibility of producing pseudo ductile FRP-by-design composite using 3D-printing technology, which leads the way to fabricate next-generation composites for civil infrastructure. Full article
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