Analysis of NMR Spectra of Submicro-Containers with Biocide DCOIT
Abstract
:1. Introduction
2. Materials and Methods
2.1. Materials
2.2. Methods
2.2.1. Preparation of SMCs
2.2.2. NMR Spectroscopy
2.2.3. SEM Scanning Electron Microscopy
3. Results and Discussion
3.1. Analysis of the NMR Spectra of the Sample DCOIT
3.2. Analysis of NMR Spectra of SMCs of TPM without Biocide in Chloroform
3.3. Analysis of NMR Spectra of SMCs of TPM with DCOIT
4. Conclusions
Author Contributions
Funding
Acknowledgments
Conflicts of Interest
References
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1H NMR Results, ppm | |||
---|---|---|---|
Sample-1 (SMCs without Biocide) | Sample-2 (SMCs with 10% DCOIT) | ∆δ = (δ0 − δ) | |
Sample-1-1 | −0.03 | −0.02 | −(−0.01) |
Sample-1-2 | 1.59 | 1.58 | −0.01 |
Sample-1-3 | 3.19 | 3.20 | 0.01 |
1H NMR Results, ppm | |||
---|---|---|---|
DCOIT in Chloroform | Sample-2 (SMCs with 10% DCOIT) | ∆δ = (δ0 − δ) | |
(DCOIT)-6 | 3.77 | 3.79 | 0.02 |
(DCOIT)-7 | 1.67 | 1.69 | 0.02 |
(DCOIT)-8,9,10,11,12 | 1.26 | 1.28 | 0.02 |
(DCOIT)-13 | 0.85 | 0.86 | 0.01 |
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Aidarova, S.B.; Issayeva, A.B.; Sharipova, A.A.; Grigoriev, D.O.; Miller, R.; Seilkhanov, T.M.; Babayev, A.A.; Issakhov, M.O. Analysis of NMR Spectra of Submicro-Containers with Biocide DCOIT. Colloids Interfaces 2020, 4, 56. https://0-doi-org.brum.beds.ac.uk/10.3390/colloids4040056
Aidarova SB, Issayeva AB, Sharipova AA, Grigoriev DO, Miller R, Seilkhanov TM, Babayev AA, Issakhov MO. Analysis of NMR Spectra of Submicro-Containers with Biocide DCOIT. Colloids and Interfaces. 2020; 4(4):56. https://0-doi-org.brum.beds.ac.uk/10.3390/colloids4040056
Chicago/Turabian StyleAidarova, Saule B., Assem B. Issayeva, Altynay A. Sharipova, Dmitry O. Grigoriev, Reinhard Miller, Tulegen M. Seilkhanov, Alpamys A. Babayev, and Miras O. Issakhov. 2020. "Analysis of NMR Spectra of Submicro-Containers with Biocide DCOIT" Colloids and Interfaces 4, no. 4: 56. https://0-doi-org.brum.beds.ac.uk/10.3390/colloids4040056