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Hydrogen, Volume 2, Issue 2 (June 2021) – 3 articles

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21 pages, 2753 KiB  
Review
Analysis of Hydrogen in Inorganic Materials and Coatings: A Critical Review
by Zdeněk Weiss
Hydrogen 2021, 2(2), 225-245; https://0-doi-org.brum.beds.ac.uk/10.3390/hydrogen2020012 - 04 Jun 2021
Cited by 10 | Viewed by 5528
Abstract
The currently used bulk analysis and depth profiling methods for hydrogen in inorganic materials and inorganic coatings are reviewed. Bulk analysis of hydrogen is based on fusion of macroscopic samples in an inert gas and the detection of the thereby released gaseous H [...] Read more.
The currently used bulk analysis and depth profiling methods for hydrogen in inorganic materials and inorganic coatings are reviewed. Bulk analysis of hydrogen is based on fusion of macroscopic samples in an inert gas and the detection of the thereby released gaseous H2 using inert gas fusion (IGF) and thermal desorption spectroscopy (TDS). They offer excellent accuracy and sensitivity. Depth profiling methods involve glow discharge optical emission spectroscopy and mass spectrometry (GDOES and GDMS), laser-induced breakdown spectroscopy (LIBS), secondary ion mass spectrometry (SIMS), nuclear reaction analysis (NRA), and elastic recoil detection analysis (ERDA). The principles of all these methods are explained in terms of the methodology, calibration procedures, analytical performance, and major application areas. The synergies and the complementarity of various methods of hydrogen analysis are described. The existing literature about these methods is critically evaluated, and major papers concerning each method are listed. Full article
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18 pages, 4171 KiB  
Article
Combined Cooling and Power Management Strategy for a Standalone House Using Hydrogen and Solar Energy
by Hugo Lambert, Robin Roche, Samir Jemeï, Pascal Ortega and Daniel Hissel
Hydrogen 2021, 2(2), 207-224; https://0-doi-org.brum.beds.ac.uk/10.3390/hydrogen2020011 - 08 May 2021
Cited by 11 | Viewed by 4075
Abstract
Tropical climate is characterized by hot temperatures throughout the year. In areas subject to this climate, air conditioning represents an important share of total energy consumption. In some tropical islands, there is no electric grid; in these cases, electricity is often provided by [...] Read more.
Tropical climate is characterized by hot temperatures throughout the year. In areas subject to this climate, air conditioning represents an important share of total energy consumption. In some tropical islands, there is no electric grid; in these cases, electricity is often provided by diesel generators. In this study, in order to decarbonize electricity and cooling production and to improve autonomy in a standalone application, a microgrid producing combined cooling and electrical power was proposed. The presented system was composed of photovoltaic panels, a battery, an electrolyzer, a hydrogen tank, a fuel cell, power converters, a heat pump, electrical loads, and an adsorption cooling system. Electricity production and storage were provided by photovoltaic panels and a hydrogen storage system, respectively, while cooling production and storage were achieved using a heat pump and an adsorption cooling system, respectively. The standalone application presented was a single house located in Tahiti, French Polynesia. In this paper, the system as a whole is presented. Then, the interaction between each element is described, and a model of the system is presented. Thirdly, the energy and power management required in order to meet electrical and thermal needs are presented. Then, the results of the control strategy are presented. The results showed that the adsorption cooling system provided 53% of the cooling demand. The use of the adsorption cooling system reduced the needed photovoltaic panel area, the use of the electrolyzer, and the use of the fuel cell by more than 60%, and reduced energy losses by 7% (compared to a classic heat pump) for air conditioning. Full article
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47 pages, 5367 KiB  
Review
Hydrogen Conversion in Nanocages
by Ernest Ilisca
Hydrogen 2021, 2(2), 160-206; https://0-doi-org.brum.beds.ac.uk/10.3390/hydrogen2020010 - 20 Apr 2021
Cited by 5 | Viewed by 3956
Abstract
Hydrogen molecules exist in the form of two distinct isomers that can be interconverted by physical catalysis. These ortho and para forms have different thermodynamical properties. Over the last century, the catalysts developed to convert hydrogen from one form to another, in laboratories [...] Read more.
Hydrogen molecules exist in the form of two distinct isomers that can be interconverted by physical catalysis. These ortho and para forms have different thermodynamical properties. Over the last century, the catalysts developed to convert hydrogen from one form to another, in laboratories and industries, were magnetic and the interpretations relied on magnetic dipolar interactions. The variety concentration of a sample and the conversion rates induced by a catalytic action were mostly measured by thermal methods related to the diffusion of the o-p reaction heat. At the turning of the new century, the nature of the studied catalysts and the type of measures and motivations completely changed. Catalysts investigated now are non-magnetic and new spectroscopic measurements have been developed. After a fast survey of the past studies, the review details the spectroscopic methods, emphasizing their originalities, performances and refinements: how Infra-Red measurements characterize the catalytic sites and follow the conversion in real-time, Ultra-Violet irradiations explore the electronic nature of the reaction and hyper-frequencies driving the nuclear spins. The new catalysts, metallic or insulating, are detailed to display the operating electronic structure. New electromagnetic mechanisms, involving energy and momenta transfers, are discovered providing a classification frame for the newly observed reactions. Full article
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