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Advances in Asphalt Materials

A special issue of Materials (ISSN 1996-1944). This special issue belongs to the section "Construction and Building Materials".

Deadline for manuscript submissions: closed (10 January 2023) | Viewed by 46310

Special Issue Editor

Prof. Dr. Marek Iwański

E-Mail Website
Guest Editor
Faculty Civil and Architectural Engineering, Kielce University of Technology, Kielce, Poland
Interests: bitumen; foamed bitumen; cold recycling; rheology; asphalt materials
Special Issues, Collections and Topics in MDPI journals

Special Issue Information

Dear Colleagues,

The need to maximise the durability and safety of road pavements is widely recognized. The main aspects that lead to durability include improving asphalt properties and developing new types of asphalt materials for pavement construction. Special attention is paid to the environmental sustainability of asphalt pavement. One of the solutions is to modify asphalt by incorporating a range of materials, such as polymers, rubber wax, F-T synthetic wax, natural asphalt, or adding various chemical additives, especially low-viscosity ones. Effectiveness of these measures is assessed with increasingly advanced rheological tests of the binder, which are capable of predicting its behaviour over pavement service life. It is very important to develop and constantly improve new types of bituminous mixtures produced with binders modified with low-viscosity additives or zeolite-foamed asphalt at lower mixing and paving temperatures (Half-Warm Mix Asphalt). From a sustainability perspective, particularly relevant are the Half-Warm Mix Asphalt technologies that rely on water-foamed asphalt and enable mixture production at a temperature of about 100 °C. In addition to a long service life, modern asphalt pavements are required to have an adequate roughness level for ensuring traffic safety. Asphalt materials such as porous asphalt or special types of SMA mixtures meet this criterion. Progressive enhancement of asphalt material properties is accompanied by advances in diagnostic methods that verify the effectiveness of the material solutions applied.

Prof. Dr. Marek Iwański
Guest Editor

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Keywords

  • modificed bitumen
  • rheology
  • asphalt materials
  • pavement diagnostics

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Published Papers (23 papers)

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Research

15 pages, 3998 KiB  
Article
Effects of Laboratory Ageing on the FTIR Measurements of Water-Foamed Bio-Fluxed Asphalt Binders
by Marek Iwański, Anna Chomicz-Kowalska, Krzysztof Maciejewski, Mateusz M. Iwański, Piotr Radziszewski, Adam Liphardt, Jan B. Król, Michał Sarnowski, Karol J. Kowalski and Piotr Pokorski
Materials 2023, 16(2), 513; https://0-doi-org.brum.beds.ac.uk/10.3390/ma16020513 - 05 Jan 2023
Cited by 3 | Viewed by 1176
Abstract
The study investigated the effects of laboratory ageing on the fluxed and water-foamed asphalt binders in scope of Fourier transform infrared spectroscopic measurements of ageing indicators and changes in their chemical composition. The investigated binders included two paving grades, two polymer modified asphalt [...] Read more.
The study investigated the effects of laboratory ageing on the fluxed and water-foamed asphalt binders in scope of Fourier transform infrared spectroscopic measurements of ageing indicators and changes in their chemical composition. The investigated binders included two paving grades, two polymer modified asphalt binders, and a highly modified asphalt binder. The bio-flux additive was produced from rapeseed methyl esters in an oxidation reaction in the presence of a metal catalyst and organic peroxide. The use of the bio-origin additive, in particular oil derivatives, was aimed at softening and better foaming of asphalt binders. This modification is possible due to the good mixability of vegetable oils with an asphalt binder, which gives a homogeneous product with reduced stiffness. The study involved the rolling thin film oven, short-term, and the pressure ageing vessel, long term, and ageing to induce oxidation on the evaluated asphalt binders. The addition of the bio-flux additive has significantly decreased the measured content of ketone compounds related to oxidation in both non-aged and aged asphalt binders, although this effect after ageing were far smaller in magnitude. Additionally, both ageing processes decreased significantly the absorbances in the ester spectral bands specific to the bio-flux additive. All mentioned effects were similar in magnitude in all tested asphalt binders. Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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11 pages, 1825 KiB  
Article
Artificial Neural Network (ANN) Modeling for Predicting Performance of SBS Modified Asphalt
by Ke Zhong, Qiao Meng, Mingzhi Sun and Guobao Luo
Materials 2022, 15(23), 8695; https://0-doi-org.brum.beds.ac.uk/10.3390/ma15238695 - 06 Dec 2022
Cited by 3 | Viewed by 1483
Abstract
Due to the superiorities of Styrene butadiene styrene (SBS) modified asphalt, it is widely used in civil engineering application. Meanwhile, accurately predicting and obtaining performance parameters of SBS modified asphalt in unison is difficult. At present, it is essential to discover an accurate [...] Read more.
Due to the superiorities of Styrene butadiene styrene (SBS) modified asphalt, it is widely used in civil engineering application. Meanwhile, accurately predicting and obtaining performance parameters of SBS modified asphalt in unison is difficult. At present, it is essential to discover an accurate and simple method between the input and output data. ANNs are used to model the performance and behavior of materials in place of conventional physical tests because of their adaptability and learning. The objective of this study discussed the application of ANNs in determining performance of SBS modified asphalt, based on attenuated total reflection Fourier transform infrared spectroscopy (ATR-FTIR) tests. A total of 150 asphalt mixtures were prepared from three matrix asphalt, two SBS modifiers and five modifier dosages. With the most suitable algorithm and number of neurons, an ANN model with seven hidden neurons was used to predict SBS content, needle penetration and softening point by using infrared spectral data of different modified asphalts as input. The results indicated that ANN-based models are valid for predicting the performance of SBS modified asphalt. The coefficient of determination (R2) of SBS content, softening point and penetration prediction models with the same grade of asphalt exceeded 99%, 98% and 96%, respectively. It can be concluded that ANNs can provide well-satisfied regression models between the SBS content and infrared spectrum statistics sets, and the precision of penetration and softening point model founded by the same grade of asphalt is high enough to can meet the forecast demand. Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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15 pages, 4331 KiB  
Article
Comparing the Effect of Thermal-Oxidation and Photo-Oxidation of Asphalt Mixtures on the Rheological and Chemical Properties of Extracted Bituminous Binder
by Ahmed Abouelsaad and Greg White
Materials 2022, 15(19), 6793; https://0-doi-org.brum.beds.ac.uk/10.3390/ma15196793 - 30 Sep 2022
Cited by 9 | Viewed by 1415
Abstract
The reliable and representative ageing of asphalt samples in the laboratory is critically important to research on asphalt durability, waste material recycling and rejuvenation treatments. However, standard laboratory ageing protocols omit ultraviolet radiation and moisture, and are also based on a universally applied [...] Read more.
The reliable and representative ageing of asphalt samples in the laboratory is critically important to research on asphalt durability, waste material recycling and rejuvenation treatments. However, standard laboratory ageing protocols omit ultraviolet radiation and moisture, and are also based on a universally applied oven temperature and ageing duration. The aim of this research was to demonstrate the importance of ultraviolet radiation in laboratory asphalt aging, motivated by the need for more realistic ageing protocols. Asphalt cores were thermally aged in a standard laboratory oven for 98 days, while other cores were aged for the same period in a weathering chamber that combined thermal–oxidative (heat) and photo-oxidative (ultraviolet irradiation) aging. The bitumen was then extracted from the top, middle and bottom of each asphalt core, and tested for rheological, chemical, and compositional properties. The results were used to compare the effects of the aging protocols, and the effects of depth below the pavement surface. It was concluded that accelerated laboratory asphalt ageing must include photo-oxidation, in combination with thermal oxidation. It was also concluded that both chemical and rheological properties were effective indicators of extracted asphalt binder aging, although the rheological testing was preferred. Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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17 pages, 3414 KiB  
Article
Quantitative Analysis of Adhesion Characteristics between Crumb Rubber Modified Asphalt and Aggregate Using Surface Free Energy Theory
by Ning Li, Jie Wang, Wei Si and Dongxia Hu
Materials 2022, 15(16), 5735; https://0-doi-org.brum.beds.ac.uk/10.3390/ma15165735 - 19 Aug 2022
Cited by 8 | Viewed by 1234
Abstract
The utilization of waste rubber tires is of great value for environment protection and resource recovery, which can also improve the properties of matrix asphalt. The adhesion characteristics were evaluated for crumb rubber modified asphalt and limestone aggregate using the surface free energy [...] Read more.
The utilization of waste rubber tires is of great value for environment protection and resource recovery, which can also improve the properties of matrix asphalt. The adhesion characteristics were evaluated for crumb rubber modified asphalt and limestone aggregate using the surface free energy (SFE) approach. Four types of matrix asphalt and four rubber contents were used to prepare the crumb rubber modified asphalt. The contact angle of matrix and crumb rubber modified asphalt was obtained, and the SFE indicators (dispersion, polar component, and compatibility rate—CR) were calculated. Moreover, the water stability tests were conducted using one matrix and rubber modified asphalt in order to investigate the relationship between SFE and water stability indicators. Results showed that the total SFE, dispersion component, adhesion work, and CR increased with the addition of crumb rubber, while the polar component and spalling work decreased. The types of asphalt had different influences on SFE indicators. The results from analysis of variation (ANOVA) indicated asphalt type and rubber content had significant influence on the adhesion work, spalling work and CR, and the influence of asphalt type was greater than that of rubber content. Additionally, the retained Marshall Stability and tensile strength ratio had better correlation with adhesion work and CR, but less with spalling work. The presented results demonstrated that the type of matrix asphalt played an important role in the adhesion characteristics for the crumb rubber modified asphalt. Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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14 pages, 4107 KiB  
Article
Influence of Type of Filler and Bitumen on the Mechanical Performance of Asphalt Mortars
by Raul Tauste-Martínez, Ana Elena Hidalgo, Gema García-Travé, Fernando Moreno-Navarro and María del Carmen Rubio-Gámez
Materials 2022, 15(9), 3307; https://0-doi-org.brum.beds.ac.uk/10.3390/ma15093307 - 05 May 2022
Cited by 4 | Viewed by 1854
Abstract
This article presents a new methodology of analysis based on a fast-running experimental procedure to characterise the mechanical response of asphalt mortars in terms of stiffness, ductility, and fatigue resistance. This was achieved using the DMA (Dynamic Mechanical Analyser) three-point bending configuration. The [...] Read more.
This article presents a new methodology of analysis based on a fast-running experimental procedure to characterise the mechanical response of asphalt mortars in terms of stiffness, ductility, and fatigue resistance. This was achieved using the DMA (Dynamic Mechanical Analyser) three-point bending configuration. The study was carried out by considering the employment of different types of fillers such cement and CaCO3 and different types of binders such as conventional asphalt binder (B35/50) or modifided polymer-modified bitumen (PMB 25/55–65). From the results of this study, the filler was found to have a greater influence on the stiffness and ductility of the asphalt material, while bitumen had a higher effect on the fatigue life of the asphalt mortar. Fatigue life was observed to increase with the use of a polymer-modified binder, while a lower degree of permanent deformation and higher bearing capacity achieved by the use of cement instead of calcium carbonate as active fillers. Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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17 pages, 1299 KiB  
Article
Gradation Design and Parameter Determination of Warm-Mix-Agent-Modified Asphalt Mixture
by Junwei Xiang, Hui Wang and Yu Xiang
Materials 2022, 15(5), 1866; https://0-doi-org.brum.beds.ac.uk/10.3390/ma15051866 - 02 Mar 2022
Viewed by 1958
Abstract
In order to make up for inadequacies such as high energy cost in the production process and quantities of waste gas and dust release of hot-mix asphalt (HMA), warm-mix asphalt (WMA) has been developed. In this paper, the preparation process of WMA mixture [...] Read more.
In order to make up for inadequacies such as high energy cost in the production process and quantities of waste gas and dust release of hot-mix asphalt (HMA), warm-mix asphalt (WMA) has been developed. In this paper, the preparation process of WMA mixture is simply introduced. According to the experimental approach of asphalt binder and asphalt mixture, EC-120 is preliminarily selected as a follow-up research object after a rheological property test and a viscosity test of five kinds of warm-mix-agent-modified asphalts combined with cost analysis. A target mix proportion of SBS~AC-16 is designed, and then through the orthogonal design of the four parameters of the Marshall test of WMA mixture, such as mixing temperature, warm-mix-agent content, compaction blows, and mixing time, the best Marshall test parameters are obtained. The results show that the best parameters are 145 °C of mixing temperature, 3% of warm-mix-agent content, 75 compaction times, and 90 s of mixing time. This study can provide technical support and reference for the construction of WMA pavement in China. Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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15 pages, 3302 KiB  
Article
Developing Hybrid Machine Learning Models to Determine the Dynamic Modulus (E*) of Asphalt Mixtures Using Parameters in Witczak 1-40D Model: A Comparative Study
by Wenjuan Xu, Xin Huang, Zhengjun Yang, Mengmeng Zhou and Jiandong Huang
Materials 2022, 15(5), 1791; https://0-doi-org.brum.beds.ac.uk/10.3390/ma15051791 - 27 Feb 2022
Cited by 20 | Viewed by 1562
Abstract
To characterize the dynamic modulus (E*) of the asphalt mixtures more accurately, a comparative study was shown in this paper, combining six ML models (BP, SVM, DT, RF, KNN, and LR) with the novelly developed MBAS (modified BAS, beetle antennae search) algorithm to [...] Read more.
To characterize the dynamic modulus (E*) of the asphalt mixtures more accurately, a comparative study was shown in this paper, combining six ML models (BP, SVM, DT, RF, KNN, and LR) with the novelly developed MBAS (modified BAS, beetle antennae search) algorithm to check the potential to replace the empirical model. The hyperparameter tuning process of the six ML models by the proposed MBAS algorithm showed satisfactory results. The calculation and evaluation process demonstrated fast convergence and significantly lower values of RMSE for the five ML models (BP, SVM, DT, RF, and KNN) to determine the E* of the asphalt mixtures. Comparing the performances of the six ML models in the prediction of the E* by the statistical coefficients and Monte Carlo simulation, the RF model showed the highest accuracy, efficiency, and robustness. Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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16 pages, 3336 KiB  
Article
Evaluating the Rheological Properties of High-Modulus Asphalt Binders Modified with Rubber Polymer Composite Modifier
by Xiaorui Zhang, Chao Han, Jun Yang, Xinquan Xu and Fan Zhang
Materials 2021, 14(24), 7727; https://0-doi-org.brum.beds.ac.uk/10.3390/ma14247727 - 14 Dec 2021
Cited by 6 | Viewed by 1914
Abstract
With the increasing traffic loading and changing climatic conditions, there is a need to use novel superior performing pavement materials such as high-modulus asphalt binders and asphalt mixtures to mitigate field distress such as rutting, cracking, etc. This laboratory study was thus conducted [...] Read more.
With the increasing traffic loading and changing climatic conditions, there is a need to use novel superior performing pavement materials such as high-modulus asphalt binders and asphalt mixtures to mitigate field distress such as rutting, cracking, etc. This laboratory study was thus conducted to explore and substantiate the usage of Rubber Polymer Composite Modifier (RPCM) for high-modulus asphalt binder modification. The base asphalt binder used in the study comprised A-70# Petroleum asphalt binder with RPCM dosages of 0.25%, 0.30%, 0.35%, 0.40% and 0.45%, separately. The laboratory tests conducted for characterizing the asphalt binder rheological and morphological properties included the dynamic mechanical analysis (DM), temperature-frequency sweep in the dynamic shear rheometer (DSR) device, bending beam rheometer (BBR), and florescence microscopic (FM) imaging. The corresponding test results exhibited satisfactory compatibility and potential for using RPCM as a high-modulus asphalt binder modifier to enhance the base asphalt binder’s rheological properties, both with respect to high- and low-temperature performance improvements. For the A-70# Petroleum asphalt binder that was evaluated, the optimum RPCM dosage was found to be 0.30–0.35%. In comparison to styrene–butadiene–styrene (SBS), asphalt binder modification with RPCM exhibited superior high-temperature rutting resistance properties (as measured in terms of the complex modulus and phase angle) and vice versa for the low-temperature cracking properties. Overall, the study beneficially contributes to the literature through provision of a reference datum toward the exploratory usage of RPCM for high-modulus asphalt binder modification and performance enhancements. Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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15 pages, 10195 KiB  
Article
Cross-Functional Test to Explore the Determination Method of Meso-Parameters in the Discrete Element Model of Asphalt Mixtures
by Xingyu Yi, Huimin Chen, Houzhi Wang, Zhiyun Tang, Jun Yang and Haopeng Wang
Materials 2021, 14(19), 5786; https://0-doi-org.brum.beds.ac.uk/10.3390/ma14195786 - 03 Oct 2021
Cited by 8 | Viewed by 1668
Abstract
In order to obtain more accurate parameters required for the simulation of asphalt mixtures in the discrete element method (DEM), this study carried out a series of cross-functional asphalt mixture experiments to obtain the DEM simulation meso-parameters. By comparing the results of simulation [...] Read more.
In order to obtain more accurate parameters required for the simulation of asphalt mixtures in the discrete element method (DEM), this study carried out a series of cross-functional asphalt mixture experiments to obtain the DEM simulation meso-parameters. By comparing the results of simulation and actual experiments, a method to obtain the meso-parameters of the DEM simulation was proposed. In this method, the numerical aggregate profile was obtained by X-ray CT scanning and the 3D aggregate model was reconstructed in MIMICS. The linear contact parameters of the aggregate and the Burgers model parameters of the asphalt mastic were obtained by nanoindentation technology. The parameters of the parallel bonding model between the aggregate and mastic were determined by the macroscopic tensile adhesion test and shear bond test. The results showed that the meso-parameters obtained by the macroscopic experiment provide a basis for the calibration of DEM parameters to a certain extent. The trends in simulation results are similar to the macro test results. Therefore, the newly proposed method is feasible. Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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35 pages, 384 KiB  
Article
Technical Challenges of Utilizing Ground Tire Rubber in Asphalt Pavements in the United States
by Rouzbeh Ghabchi, Amir Arshadi, Musharraf Zaman and Ferrella March
Materials 2021, 14(16), 4482; https://0-doi-org.brum.beds.ac.uk/10.3390/ma14164482 - 10 Aug 2021
Cited by 10 | Viewed by 2658
Abstract
At least 275 million scrap tires exist in stockpiles in the U.S. The practice of dumping scrap tires in landfills has been an environmental concern. To address this concern, many industries—and regional and national environmental protection agencies—have taken major initiatives to recycle scrap [...] Read more.
At least 275 million scrap tires exist in stockpiles in the U.S. The practice of dumping scrap tires in landfills has been an environmental concern. To address this concern, many industries—and regional and national environmental protection agencies—have taken major initiatives to recycle scrap tires. One of the major uses of recycled scrap tires is in crumb rubber products, including rubberized asphalt. Rubberized asphalt is produced by blending ground tire rubber with asphalt to beneficially modify its properties for highway construction. The ground tire rubber (GTR) can be used either as part of the asphalt rubber binder (also known as asphalt rubber), seal coat, cap seal spray, joint and crack sealant or as substitute aggregate (rubber-modified asphalt concrete). Therefore, the largest single market for GTR is asphalt rubber, which consumes approximately 12 million tires, annually. Currently, several Departments of Transportation (DOTs) in the U.S. do not allow use of GTR in asphalt mixes. This is partly due to lack of information, laboratory test data and specifications or special provisions on the use of GTR in asphalt pavements. The current study was undertaken to summarize the available wealth of knowledge, identify research needs, and document the major findings of previous pertinent studies focused on GTR use in asphalt. Significant study findings—consisting of laboratory test results, field observations, and common practices—were documented, including: the use of GTR in asphalt mixes, wet and dry processes, characterization of hot mix asphalt (HMA) containing GTR and GTR performance when combined with virgin materials. In order to promote successful use of GTR, it is imperative to help DOTs develop specifications/special provisions for utilizing rubberized asphalt by collecting data, common practices and specifications utilized by other state DOTs. As a part of this effort, we conducted a survey of construction specifications used by different DOTs that currently allow the use of GTR in asphalt. Since some DOT practices are not readily available in the open literature, this survey proved to be an effective tool for gathering data on the current practices, methods and specifications associated with DOT use of GTR in asphalt pavement. Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
12 pages, 2733 KiB  
Article
Performance Evaluation of Warm Asphalt Mixtures Containing Chemical Additive and Effect of Incorporating High Reclaimed Asphalt Content
by Mukul Rathore, Viktors Haritonovs and Martins Zaumanis
Materials 2021, 14(14), 3793; https://0-doi-org.brum.beds.ac.uk/10.3390/ma14143793 - 07 Jul 2021
Cited by 17 | Viewed by 2701
Abstract
Reclaimed asphalt (RA) and Warm mix asphalt (WMA) are two widely used environmentally friendly mixtures in the paving industry. This study compares the laboratory performance of conventional hot mix asphalt (HMA) with virgin WMA, and WMA containing 60% RA content, using thermal stress [...] Read more.
Reclaimed asphalt (RA) and Warm mix asphalt (WMA) are two widely used environmentally friendly mixtures in the paving industry. This study compares the laboratory performance of conventional hot mix asphalt (HMA) with virgin WMA, and WMA containing 60% RA content, using thermal stress restrained specimen test, wheel tracking test, and indirect tensile strength test. Based on test results, a reduction of 15 °C in mixing temperature was achieved for WMA mixtures compared to HMA using the given chemical additive. The virgin WMA mixture showed superior cracking resistance but lower rutting resistance than HMA, and incorporation of RA material without any further modification in the binder, deteriorated both cracking and rutting performance of WMA. It was also shown that laboratory short-term aging can significantly affect the performance of the mixtures. Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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14 pages, 14663 KiB  
Article
Investigation of Mechanical and Hydrologic Characteristics of Porous Asphalt Pavement with a Geocell Composite
by Jaehun Ahn, Tan Hung Nguyen, In Kyoon Yoo and Jeongho Oh
Materials 2021, 14(12), 3165; https://0-doi-org.brum.beds.ac.uk/10.3390/ma14123165 - 09 Jun 2021
Cited by 6 | Viewed by 2282
Abstract
Porous asphalt pavement is a part of the permeable pavement system, which can be used to mitigate the negative impacts of urbanisation on the water hydrological cycle and environment. This study aims to assess the mechanical and hydrologic characteristics of porous asphalt pavements, [...] Read more.
Porous asphalt pavement is a part of the permeable pavement system, which can be used to mitigate the negative impacts of urbanisation on the water hydrological cycle and environment. This study aims to assess the mechanical and hydrologic characteristics of porous asphalt pavements, with and without geocell composites, using a plate load test, falling weight deflectometer test, and rainfall simulation test. The corresponding results indicate that the elastic modulus of the unreinforced pavement is lower than that of the reinforced pavement. The analysis demonstrates that the use of geocell composites effectively increases the load-bearing capacity of the pavement. When the base layer is reinforced with geocells, its load-bearing capacity increases. Observation of the rainfall simulation tests on the reinforced pavement indicates that the reinforced pavement effectively handles the surface runoff. Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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14 pages, 3406 KiB  
Article
Study on Performance Damage and Mechanism Analysis of Asphalt under Action of Chloride Salt Erosion
by Peilei Zhou, Wensheng Wang, Lili Zhu, Haoyun Wang and Yongming Ai
Materials 2021, 14(11), 3089; https://0-doi-org.brum.beds.ac.uk/10.3390/ma14113089 - 04 Jun 2021
Cited by 17 | Viewed by 1765
Abstract
This study aims to investigate the performance evolution and mechanism of asphalt under action of chloride salt erosion. Asphalt samples soaked with five different snow melting chloride salt concentrations were taken as the research object. Then, the high-temperature performance, low-temperature performance, temperature sensitivity [...] Read more.
This study aims to investigate the performance evolution and mechanism of asphalt under action of chloride salt erosion. Asphalt samples soaked with five different snow melting chloride salt concentrations were taken as the research object. Then, the high-temperature performance, low-temperature performance, temperature sensitivity and asphalt–aggregate adhesion property of asphalt samples were carried out. Additionally, Fourier transform infrared spectroscopy (FTIR) was used to explore the mechanism of chloride salt erosion on asphalt. Test results showed the linear variation relationships of high-temperature performance, low-temperature performance and temperature sensitivity with chloride salt concentrations. The high-temperature performance of asphalt would be improved by chloride snowmelt salt. With the increase in the chloride salt solution concentration, the low-temperature performance of asphalt became worse, and the temperature sensitivity increased. Moreover, after the effect of the chloride salt solution, the asphalt–aggregate adhesion property decreased with the increase in the chloride salt solution concentration. It is necessary to control the amount of chloride snowmelt salt in the actual snow removal projects. Finally, based on Fourier transform infrared spectroscopy, the mechanism of chloride salt erosion on asphalt was preliminarily explored. With the increase in the chloride salt solution concentration, the proportion of light components (saturated fraction, aromatic fraction) in asphalt decreased, and the proportion of heavy components (resin and asphaltene) with good thermal stability increased. Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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18 pages, 7147 KiB  
Article
Investigation of Acoustic Properties of Poroelastic Asphalt Mixtures in Laboratory and Field Conditions
by Wladyslaw Gardziejczyk, Piotr Jaskula, Jerzy A. Ejsmont, Marek Motylewicz, Marcin Stienss, Piotr Mioduszewski, Pawel Gierasimiuk and Maciej Zawadzki
Materials 2021, 14(10), 2649; https://0-doi-org.brum.beds.ac.uk/10.3390/ma14102649 - 18 May 2021
Cited by 8 | Viewed by 1842
Abstract
Measures for the improvement of acoustic conditions in the vicinity of roads include the construction of pavement structures with low-noise surfaces with optimal macrotexture and the highest possible sound absorption coefficient. Laboratory evaluation of acoustic properties of a designed asphalt mixture before its [...] Read more.
Measures for the improvement of acoustic conditions in the vicinity of roads include the construction of pavement structures with low-noise surfaces with optimal macrotexture and the highest possible sound absorption coefficient. Laboratory evaluation of acoustic properties of a designed asphalt mixture before its placement in the pavement is a good solution. Currently, the most popular method for the determination of the sound absorption coefficient of various construction materials under laboratory conditions is the Kundt’s tube test. Sound absorption coefficient can also be assessed based on field and laboratory measurements performed using a Spectronics ACUPAVE System. Other parameters characterising the acoustic properties of road pavement courses include air void content and water drainability or permeability. The article presents an analysis of results of sound absorption coefficient obtained using a Spectronics ACUPAVE System and water drainability and permeability of poroelastic mixtures obtained both in laboratory and on test sections, in relation to air void content and grading of the mixtures. It was established that poroelastic mixtures containing an aggregate of maximum particle size of 5 mm are characterised by better acoustic properties than mixtures with a maximum aggregate particle size of 8 mm. Changes of crumb rubber aggregate grading and bitumen type (within the tested range of values) as well as the addition of lime have shown no evident influence on the sound absorption coefficient. Noise level values at the speed of 30 km/h according to the CPX method were measured as well. Relationships between sound absorption coefficient, water drainability/permeability, and air void content were determined. The performed analyses confirmed that Spectronics ACUPAVE System may be applied for evaluation of acoustic properties of asphalt mixtures in laboratory conditions, but further research is needed to reduce the uncertainty of the results. Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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14 pages, 641 KiB  
Article
Calculation Method of Permanent Deformation of Asphalt Mixture Based on Interval Number
by Yue Xiao, Limin Tang and Jiawei Xie
Materials 2021, 14(9), 2116; https://0-doi-org.brum.beds.ac.uk/10.3390/ma14092116 - 22 Apr 2021
Cited by 1 | Viewed by 1284
Abstract
There are great uncertainties in road design parameters, and the traditional point numerical calculation results cannot reflect the complexity of the actual project well. Additionally, the calculation method of road design theory based on interval analysis is more difficult in the use of [...] Read more.
There are great uncertainties in road design parameters, and the traditional point numerical calculation results cannot reflect the complexity of the actual project well. Additionally, the calculation method of road design theory based on interval analysis is more difficult in the use of uncertain design parameters. In order to simplify the calculation process of the interval parameters in the road design theory, the asphalt pavement design is taken as the analysis object, and the permanent deformation of the asphalt mixture is simplified by combining the interval analysis theory. Considering the uncertainty of the design parameters, the data with boundaries but uncertain size are expressed in intervals, and then the interval calculation formula for the permanent deformation of the asphalt mixture is derived, and the interval results are obtained. In order to avoid the dependence of interval calculation on the computer code, according to the interval calculation rule, the interval calculation method with the upper and lower end point values as point operations is proposed. In order to overcome the contradiction between interval expansion results and engineering applications, by splitting the multi-interval variable formulas, the interval variable weights are reasonably given, and the synthesis of each single interval result realizes a simplified calculation based on interval variable weight assignment. The analysis results show that the interval calculation method based on the point operation rule is accurate and reliable, and the simplified method based on the interval variable weight assignment is effective and feasible. The simplified interval calculation method proposed in this paper provides a reference for the interval application of road design theory. Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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14 pages, 3737 KiB  
Article
Laboratory Characterization of Porous Asphalt Mixtures with Aramid Fibers
by Anik Gupta, Pedro Lastra-Gonzalez, Daniel Castro-Fresno and Jorge Rodriguez-Hernandez
Materials 2021, 14(8), 1935; https://0-doi-org.brum.beds.ac.uk/10.3390/ma14081935 - 13 Apr 2021
Cited by 13 | Viewed by 1963
Abstract
Recent studies have shown that fibers improve the performance of porous asphalt mixtures. In this study, the influence of four different fibers, (a) regular aramid fiber (RegAR), (b) aramid fiber with latex coating (ARLat), (c) aramid fiber with polyurethane coating (ARPoly), (d) aramid [...] Read more.
Recent studies have shown that fibers improve the performance of porous asphalt mixtures. In this study, the influence of four different fibers, (a) regular aramid fiber (RegAR), (b) aramid fiber with latex coating (ARLat), (c) aramid fiber with polyurethane coating (ARPoly), (d) aramid fiber of length 12 mm (AR12) was evaluated on abrasion resistance and toughness of the mixtures. The functional performance was estimated using permeability tests and the mechanical performance was evaluated using the Cantabro test and indirect tensile strength tests. The parameters such as fracture energy, post cracking energy, and toughness were obtained through stress-strain plots. Based on the analysis of results, it was concluded that the addition of ARLat fibers enhanced the abrasion resistance of the mixtures. In terms of ITS, ARPoly and RegAR have positively influenced mixtures under dry conditions. However, the mixtures with all aramid fibers were found to have adverse effects on the ITS under wet conditions and energy parameters of porous asphalt mixtures with the traditional percentages of bitumen in the mixture used in Spain (i.e., approximately 4.5%). Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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22 pages, 11807 KiB  
Article
Experimental Study of Tensile Properties of Styrene–Butadiene–Styrene Modified Asphalt Binders
by Paweł Mieczkowski, Bartosz Budziński, Mieczysław Słowik, Jan Kempa and Wojciech Sorociak
Materials 2021, 14(7), 1734; https://0-doi-org.brum.beds.ac.uk/10.3390/ma14071734 - 01 Apr 2021
Cited by 10 | Viewed by 2183
Abstract
The requirements imposed on road pavements are ever increasing nowadays, necessitating the improvement of the properties of paving materials. The most commonly used paving materials include bituminous mixtures that are composed of aggregate grains bound by a bituminous binder. The properties of bitumens [...] Read more.
The requirements imposed on road pavements are ever increasing nowadays, necessitating the improvement of the properties of paving materials. The most commonly used paving materials include bituminous mixtures that are composed of aggregate grains bound by a bituminous binder. The properties of bitumens can be improved by modification with polymers. Among the copolymers used for modifying bitumens, styrene–butadiene–styrene, a thermoplastic elastomer, is the most commonly used. This article presents the results of tests conducted on bitumens modified with two types of styrene–butadiene–styrene copolymer (linear and radial). Two bitumen types of different penetration grades (35/50 and 160/220) were used in the experiments. The content of styrene–butadiene–styrene added to the bitumen varied between 1% and 6%. The results of the force ductility test showed that cohesion energy can be used for qualitative evaluation of the efficiency of modification of bitumen with styrene–butadiene–styrene copolymer. The determined values of the cohesion energy were subjected to the original analysis taking into account the three characteristic elongation zones of the tested binders. The performed analyses made it possible to find a parameter whose values correlate significantly with the content of styrene–butadiene–styrene copolymer in the modified bitumen. With smaller amounts of added modifier (approximately 2%), slightly better effects were obtained in the case of linear copolymer styrene–butadiene–styrene and for larger amounts of modifier (5–6%) radial copolymer styrene–butadiene–styrene was found to be more effective. This is confirmed by the changes in the binder structure, as indicated by the penetration index (PI). Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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20 pages, 4614 KiB  
Article
Study on Rheological Properties of Bituminous Binders and Mixtures Containing Waste Printed Circuit Boards (PCBs) and SBR Compound Modified Bitumen
by Yongjun Meng, Yongjie Liao, Zhirong Liu, Jing Chen, Xiaolong Yang and Hongliu Rong
Materials 2021, 14(7), 1697; https://0-doi-org.brum.beds.ac.uk/10.3390/ma14071697 - 30 Mar 2021
Cited by 5 | Viewed by 1909
Abstract
Improper handling of waste printed circuit boards (PCBs) can cause serious pollution to the water and soil environments. In order to explore a new method of recycling waste PCBs, this study investigated the effect of PCBs and butadiene styrene rubber (SBR) on the [...] Read more.
Improper handling of waste printed circuit boards (PCBs) can cause serious pollution to the water and soil environments. In order to explore a new method of recycling waste PCBs, this study investigated the effect of PCBs and butadiene styrene rubber (SBR) on the rheological properties of neat bitumen. The dynamic shear rheological (DSR) test was used to study the effect of different PCB contents on the high-temperature rheological properties of SBR-modified bitumen. Fluorescence microscopy and Fourier-transform infrared spectroscopy were used to study the microstructure change law and modification mechanism of PCB and SBR composite modified bitumen. Finally, the feasibility of the bitumen properties was verified through a test of the bituminous mixture properties. The DSR test results showed that the addition of PCBs improves the elastic recovery modulus, dynamic shear modulus, and rutting factor of SBR-modified bitumen, indicating that the high-temperature properties were improved. Infrared spectroscopy analysis revealed that a new absorption peak was generated in the infrared spectrum of the compound bitumen after the addition of PCBs, and the intensity of the original absorption peak also changed, indicating that PCBs and SBR-modified bitumen were mainly physically blended and accompanied by a weak chemical reaction. It was further found that the absorption peak of the unsaturated C=C double bond was significantly enhanced, and the increase in the content of the unsaturated bond C=C in the main chain of the polymer significantly increases the stiffness of the bitumen. Macroscopically, the high-temperature rutting resistance was improved to a certain extent. The fluorescence diagram shows that when PCBs do not exceed 10%, the PCBs can form a homogeneous structure and be dispersed in SBR-modified bitumen. The road test of PCBs and SBR composite modified bituminous mixtures showed that PCBs can significantly improve the rutting resistance and water stability of SBR-modified bitumen at high temperatures at the recommended optimum content. The crack resistance at low temperatures is weakened but still meets actual engineering requirements. The correlation analysis between the properties of bitumen and bituminous mixtures is carried out based on grey correlation theory. The results show that the index of modified bitumen has a very good guiding effect on the bituminous mixture properties. The development of PCBs and SBR composite-modified bitumen provides a new practical method for recycling waste PCBs. Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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22 pages, 59447 KiB  
Article
Influence of Compound Modification of Oil Sands De-Oiled Asphalt and Polyphosphoric Acid on High- and Low-Temperature Performance of Styrene-Butadiene-Styrene-Modified Asphalt
by Xiaoguang Pei and Weiyu Fan
Materials 2021, 14(4), 797; https://0-doi-org.brum.beds.ac.uk/10.3390/ma14040797 - 08 Feb 2021
Cited by 5 | Viewed by 1916
Abstract
Oil sands de-oiled asphalt (OSDOA) has become a bottleneck for refineries due to its enormous production and huge landfill costs. Applying OSDOA as a modifier is an effective way to reduce environmental pollution and disposal cost. In this study, the influences of OSDOA [...] Read more.
Oil sands de-oiled asphalt (OSDOA) has become a bottleneck for refineries due to its enormous production and huge landfill costs. Applying OSDOA as a modifier is an effective way to reduce environmental pollution and disposal cost. In this study, the influences of OSDOA and polyphosphoric acid (PPA) compound modification on styrene-butadiene-styrene (SBS)-modified binder were investigated. The high-temperature rutting resistance, low-temperature anti-crack performance and fatigue resistance were obtained by dynamic shear rheometer (DSR) and bending beam rheometer (BBR) test. Storage stability and microstructure were also investigated by storage test and Fourier-transform infrared (FTIR) spectroscopy. The results demonstrated that the compound modification of OSDOA/PPA dramatically enhanced the deformation resistance of SBS-modified binder and reduced its low-temperature cracking resistance. The anti-fatigue performance was also decreased. Moreover, the combined effect of OSDOA and PPA could produce composite modified asphalt with excellent storage stability, which was verified by desirable fluorescence images. Furthermore, both physical and chemical interactions coexisted during the OSDOA/PPA compound modification process. Consequently, the optimal doses of OSDOA and PPA were determined to be 10 wt% and 1.0 wt%, considering of the balance between high- and low-temperature characteristics and storage stability of composite modified asphalt. Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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18 pages, 2444 KiB  
Article
Laboratory Evaluation of the Performance of Stone Mastic Asphalt as an Ungrooved Runway Surface
by Sean Jamieson and Greg White
Materials 2021, 14(3), 502; https://0-doi-org.brum.beds.ac.uk/10.3390/ma14030502 - 21 Jan 2021
Cited by 3 | Viewed by 1951
Abstract
Many airports are surfaced with grooved Marshall-designed dense graded asphalt. Grooving is required to satisfy regulatory aircraft skid resistance requirements, but introduces the risk of groove-related distress, such as groove closure. Consequently, airports seek an ungrooved runway surface option that performs similarly to [...] Read more.
Many airports are surfaced with grooved Marshall-designed dense graded asphalt. Grooving is required to satisfy regulatory aircraft skid resistance requirements, but introduces the risk of groove-related distress, such as groove closure. Consequently, airports seek an ungrooved runway surface option that performs similarly to dense graded asphalt but allows grooving to be avoided. Stone mastic asphalt is the most viable ungrooved runway surface solution and has been used on runways in Europe and China. However, before being accepted as an ungrooved runway surface in Australia, stone mastic asphalt must be shown to meet regulatory runway aircraft skid resistance requirements, and to otherwise perform similarly to typical dense graded asphalt mixtures for runway surfacing, including deformation resistance, fatigue cracking resistance and durability. Based on laboratory performance-related testing, 10-mm and 14-mm sized stone mastic asphalt mixtures, produced with four different aggregate sources, were found to generally meet the airport asphalt performance requirements. The 14 mm mixture was found to perform better than the 10 mm mixture, particularly regarding surface macrotexture and deformation resistance. It was concluded that airports should consider 14 mm sized stone mastic asphalt as an ungrooved runway surface in the future. Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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23 pages, 9714 KiB  
Article
Molecular Dynamic Investigations on the Adhesion Behaviors of Asphalt Mastic–Aggregate Interface
by Wenyi Xu, Xin Qiu, Shanglin Xiao, Ganghua Hu, Feng Wang and Jie Yuan
Materials 2020, 13(22), 5061; https://0-doi-org.brum.beds.ac.uk/10.3390/ma13225061 - 10 Nov 2020
Cited by 16 | Viewed by 2596
Abstract
The asphalt mastic–aggregate interface plays an essential role in determining the service performance of asphalt mixtures. The objective of this paper was to investigate the adhesion behaviors and mechanism between asphalt mastic and aggregate based on molecular dynamic (MD) simulations. First, the asphalt [...] Read more.
The asphalt mastic–aggregate interface plays an essential role in determining the service performance of asphalt mixtures. The objective of this paper was to investigate the adhesion behaviors and mechanism between asphalt mastic and aggregate based on molecular dynamic (MD) simulations. First, the asphalt mastic model considering the actual mass ratio of filler to asphalt (F/A) condition was established and validated in terms of thermodynamic properties. Second, the molecular arrangement characteristics of polar components on the aggregate substrate were analyzed by radial distribution function (RDF), relative concentration (RC), and mean square displacement (MSD). Third, the interfacial adhesion ability between asphalt and aggregate was quantitively evaluated based on the work of adhesion. Finally, the coupling effect of moisture and temperature on interfacial adhesion behaviors was investigated to explore the adhesion failure characteristics of the asphalt–aggregate interface. The results demonstrate that the thermodynamic properties could be employed to validate the reliability of the asphalt mastic model. The self-aggregation degree of polar components in base asphalt could be significantly increased with the addition of silica particles, exhibiting a change of configuration from “parallel arrangement” into “stack distribution” due to the high polarity of silica particles. The polar components in asphalt mastic exhibit a more uniform distribution state and lower mobility capability than base asphalt owing to the adsorption effect of silica particles. Silica particles with amounts of residual charges could significantly increase the electrostatic energy of the asphalt mastic–aggregate interface, contributing to an improvement of the adhesion between asphalt mastic and aggregate. The increase of temperature enhances the work of adhesion of the asphalt mastic–aggregate interface, which is opposite to that of the base asphalt–aggregate interface. The asphalt mastic exhibits a greater sensitivity to interfacial moisture damage than base asphalt. The findings would provide insights into a better understanding on the micro adhesion mechanism of the asphalt mastic–aggregate interface. Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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26 pages, 4065 KiB  
Article
Predict the Phase Angle Master Curve and Study the Viscoelastic Properties of Warm Mix Crumb Rubber-Modified Asphalt Mixture
by Fei Zhang, Lan Wang, Chao Li and Yongming Xing
Materials 2020, 13(21), 5051; https://0-doi-org.brum.beds.ac.uk/10.3390/ma13215051 - 09 Nov 2020
Cited by 13 | Viewed by 2658
Abstract
To identify the most accurate approach for constructing of the dynamic modulus master curves for warm mix crumb rubber modified asphalt mixtures and assess the feasibility of predicting the phase angle master curves from the dynamic modulus ones. The SM (Sigmoidal model) and [...] Read more.
To identify the most accurate approach for constructing of the dynamic modulus master curves for warm mix crumb rubber modified asphalt mixtures and assess the feasibility of predicting the phase angle master curves from the dynamic modulus ones. The SM (Sigmoidal model) and GSM (generalized sigmoidal model) were utilized to construct the dynamic modulus master curve, respectively. Subsequently, the master curve of phase angle could be predicted from the master curve of dynamic modulus in term of the K-K (Kramers–Kronig) relations. The results show that both SM and GSM can predict the dynamic modulus very well, except that the GSM shows a slightly higher correlation coefficient than SM. Therefore, it is recommended to construct the dynamic modulus master curve using GSM and obtain the corresponding phase angle master curve in term of the K-K relations. The Black space diagram and Wicket diagram were utilized to verify the predictions were consistent with the LVE (linear viscoelastic) theory. Then the master curve of storage modulus and loss modulus were also obtained. Finally, the creep compliance and relaxation modulus can be used to represent the creep and relaxation properties of warm-mix crumb rubber-modified asphalt mixtures. Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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29 pages, 3940 KiB  
Article
The Discrete and Continuous Retardation and Relaxation Spectrum Method for Viscoelastic Characterization of Warm Mix Crumb Rubber-Modified Asphalt Mixtures
by Fei Zhang, Lan Wang, Chao Li and Yongming Xing
Materials 2020, 13(17), 3723; https://0-doi-org.brum.beds.ac.uk/10.3390/ma13173723 - 23 Aug 2020
Cited by 10 | Viewed by 2404
Abstract
To study the linear viscoelastic (LVE) of crumb rubber-modified asphalt mixtures before and after the warm mix additive was added methods of obtaining the discrete and continuous spectrum are presented. Besides, the relaxation modulus and creep compliance are constructed from the discrete and [...] Read more.
To study the linear viscoelastic (LVE) of crumb rubber-modified asphalt mixtures before and after the warm mix additive was added methods of obtaining the discrete and continuous spectrum are presented. Besides, the relaxation modulus and creep compliance are constructed from the discrete and continuous spectrum, respectively. The discrete spectrum of asphalt mixtures can be obtained from dynamic modulus test results according to the generalized Maxwell model (GMM) and the generalized Kelvin model (GKM). Similarly, the continuous spectrum of asphalt mixtures can be obtained from the dynamic modulus test data via the inverse integral transformation. In this paper, the test procedure for all specimens was ensured to be completed in the LVE range. The results show that the discrete spectrum and the continuous spectrum have similar shapes, but the magnitude and position of the spectrum peaks is different. The continuous spectrum can be considered as the limiting case of the discrete spectrum. The relaxation modulus and creep compliance constructed by the discrete and continuous spectrum are almost indistinguishable in the reduced time range of 10−5 s–103 s. However, there are more significant errors outside the time range, and the maximum error is up to 55%. Full article
(This article belongs to the Special Issue Advances in Asphalt Materials)
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