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Mechanical Alloying and Powder Compaction of Crystalline and Amorphous Composites

A special issue of Materials (ISSN 1996-1944). This special issue belongs to the section "Metals and Alloys".

Deadline for manuscript submissions: closed (10 December 2022) | Viewed by 2123

Special Issue Editor


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Guest Editor
Faculty of Materials Science and Engineering, Warsaw University of Technology, 141 Woloska Str., 02-507 Warsaw, Poland
Interests: mechanical alloying; mechanosynthesis; amorphous alloys; nanostructured materials; metallic and ceramic composites; metallic glasses; bulk metallic glasses; high-entropy alloys; powder compaction; X-ray diffraction; thermal stability

Special Issue Information

Dear Colleagues,

Mechanical alloying is widely recognized as a powder processing technique leading to the formation of many non-equilibrium and equilibrium structures, like extended solid solutions, amorphous alloys, nanocrystalline (nanostructured) alloys, intermetallic compounds, or in situ composites. There are many modifications to the process, depending on the nature of the transformation (alloying, milling, mechanochemical reaction). However, the final phase composition and structure always depend on thermodynamic (e.g., mutual solubility of the elements, enthalpy of mixing, differences in atomic radii) and processing (e.g., type of mill, energy of milling, ball-to-powder weight ratio, process control agent) parameters.

The next step following the mechanical alloying process is usually powder compaction, preserving their non-equilibrium structure. Various techniques are employed for powder consolidation, like cold pressing followed by sintering, hot pressing, hot isostatic pressing, explosive compaction, and spark plasma sintering. In many cases, amorphous powder compaction is an alternative to the rapid quenching (casting) technique, which can obtain bulk amorphous alloys and their composites. Compaction of mechanically alloyed powders/composites can also help to overcome many problems related to the traditional manufacturing of metal matrix composites, like particle agglomeration, low wettability, or interfacial reactions.

This Special Issue of Materials will be a detailed overview of recent research and development in the field of mechanical alloying/milling of metallic/ceramic powders followed by their compaction to get bulk amorphous/nanocrystalline materials and composites.

It is my pleasure to invite you to submit a manuscript for this Special Issue. Full papers, communications, and reviews related to mechanical alloying and powder compaction are all welcome.

Prof. Dariusz Oleszak
Guest Editor

Manuscript Submission Information

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Submitted manuscripts should not have been published previously, nor be under consideration for publication elsewhere (except conference proceedings papers). All manuscripts are thoroughly refereed through a single-blind peer-review process. A guide for authors and other relevant information for submission of manuscripts is available on the Instructions for Authors page. Materials is an international peer-reviewed open access semimonthly journal published by MDPI.

Please visit the Instructions for Authors page before submitting a manuscript. The Article Processing Charge (APC) for publication in this open access journal is 2600 CHF (Swiss Francs). Submitted papers should be well formatted and use good English. Authors may use MDPI's English editing service prior to publication or during author revisions.

Keywords

  • Mechanical alloying
  • Mechanical milling
  • Mechanochemical reactions
  • Amorphous and nanocrystalline powders
  • Bulk amorphous and nanostructured alloys
  • Metallic composites
  • Ceramic composites
  • Powder compaction

Published Papers (1 paper)

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Research

13 pages, 7640 KiB  
Article
Al13Fe4-Al Composites with Nanocrystalline Matrix Manufactured by Hot-Pressing of Milled Powders
by Marek Krasnowski, Stanislaw Gierlotka and Dariusz Zasada
Materials 2022, 15(12), 4241; https://0-doi-org.brum.beds.ac.uk/10.3390/ma15124241 - 15 Jun 2022
Viewed by 1107
Abstract
The paper describes composites with the matrix containing a nanocrystalline intermetallic Al13Fe4 phase and microcrystalline aluminium. Mechanically alloyed Al80Fe20 powder, containing a metastable nanocrystalline Al5Fe2 phase, was mixed with 20, 30, and 40 vol.% [...] Read more.
The paper describes composites with the matrix containing a nanocrystalline intermetallic Al13Fe4 phase and microcrystalline aluminium. Mechanically alloyed Al80Fe20 powder, containing a metastable nanocrystalline Al5Fe2 phase, was mixed with 20, 30, and 40 vol.% of Al powder and consolidated at 750 °C under the pressure of 7.7 GPa. During the consolidation, the metastable Al5Fe2 phase transformed into a nanocrystalline Al13Fe4 phase. In the bulk samples, Al13Fe4 areas were wrapped around by networking Al regions. The hardness of the Al13Fe4-Al composites was in the range of 4.52–5.50 GPa. The compressive strength of the Al13Fe4-30%Al and Al13Fe4-40%Al composites was 805 and 812 MPa, respectively, and it was considerably higher than that of the Al13Fe4-20%Al composite (538 MPa), which failed in the elastic region. The Al13Fe4-30%Al and Al13Fe4-40%Al composites, in contrast, showed some plasticity: namely, 1.5% and 9.1%, respectively. The density of the produced composites is in the range of 3.27–3.48 g/cm3 and decreases with the increase in the Al content. Full article
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