1. Introduction
Stone mastic asphalt (SMA) [
1,
2] has been widely used in the construction of highways because of its excellent engineering performances. SMA has a high coarse aggregate content that interlocks to form a stone skeleton that resists permanent deformation. The stone skeleton is filled with a mastic of bitumen and filler. It has more stone-on-stone contact and asphalt content than conventional dense graded asphalt mixtures [
1,
2]. However, with the continuous growth of the logistics industry and traffic load, many asphalt mixtures suffer early damage within 1 to 2 years of service, and in this respect, the durability of the mixtures is gaining increasing attention from the people [
3,
4]. Thus, researchers hope to further improve the performance of SMA pavement by using various additives [
5,
6,
7], in which high-quality fiber is an important one.
At present, the common fibers in SMA include plant fiber, polymer synthetic fiber, glass fiber, and so on [
8]. Lignin fiber (LF) is the most widely used in SMA [
8]. Other similar fibers, such as straw composite fiber [
9], bamboo fiber [
10], and cellulose fiber [
11], were also evaluated for SMA. Such plant fibers could absorb extra free asphalt. However, some researchers argued that the asphalt absorbed by these fibers is just a waste of money because the absorbed asphalt does not contribute to the mixture strength [
12]. Additionally, these plant fibers may lose the ability to absorb free asphalt gradually because it could degrade due to the oxidation during the service life [
13,
14]. Apart from plant fibers, many researchers have studied kinds of polymer synthetic fibers for SMA, such as polyester fiber, polypropylene fiber, and so on [
15,
16,
17]. They believe that polymer fibers and asphalt are chemically similar and that they can synergize well with the forces. However, some researchers have found that polymer fibers tend to curl at high temperatures, which weakens their function in the mixtures. [
9] Additionally, glass fiber is another type of stabilizers used for SMA. Some researchers concluded that fatigue behavior of asphalt concrete reinforced by glass fiber exhibits positive influences [
18,
19]. Some researchers also found that the brittleness of glass fibers causes it to break easily when mixed with mineral aggregates [
20], and the smooth surface of glass fiber leads to poor adhesion with asphalt.
Basalt fiber (BF) is a new kind of inorganic fiber developing in recent years [
21,
22]. It is made from basalt stone at 1450 °C, and the production process does not produce any harmful by-products. Nowadays, BF has been paid more and more attention in the asphalt pavement engineering due to its excellent technical performance and environmental benefits [
23,
24,
25]. Liu found that basalt fiber can better improve the performance of SMA-13 mixture than other fibers [
26]. Cheng [
27] concluded that the addition of basalt fiber is the main reason of improving the mixture performance. Wang [
28] found that basalt fiber can effectively reduce the damage degree of asphalt mixture in freeze–thaw cycle test.
Many useful conclusions have been achieved in the study of fresh BF asphalt mixtures. However, more and more attention has been paid to its long-term performance. Although Lee [
29], Enieb [
30] have evaluated the long-term performance of glass fiber asphalt mixtures, more studies on the effect of different fibers on the long-term performance of SMA are needed. Therefore, this paper focuses on the study on the long-term performances of SMA containing different fibers. BFSMA-13(defined as the SMA-13 containing BF) and LFSMA-13 (defined as the SMA-13 containing BF) were designed for test. The high-temperature performance, low-temperature property, water stability, and anti-cracking ability of mixtures under different aging degrees (unaged, short-erm aged, and long-term aged) were compared and analyzed. SEM tests were adopted to analyze the distribution of BF and LF in the mixture to reveal the strengthening mechanism of the fibers. Since fibers are needed in SMA-13 to stabilize free asphalt [
8], hence the SMA-13 without fibers are not manufactured in this study, and LFSMA-13 can be treated as standard SMA-13 in this article. The findings of this study help to further understand the performance changes of SMA-13 mixtures during the service life and to guide the selection of fiber additives for SMA-13 mixtures.
3. Test Scope and Methods
In this paper, the effect of fiber types on the performance of SMA under different aged states was explored. First, mixture specimen under different aged states were fabricated. The short-term aged mixtures were used to simulate asphalt mixtures during construction, and the long-term aged mixtures were prepared to simulate asphalt mixtures that have been paved for five to seven years. The aged BFSMA-13 and LFSMA-13 were prepared following the steps provided by AASHTO R30 [
32]. Then, the performances of these specimen were checked with several test methods. The wheel tracking test and the uniaxial penetration test were adopted to reveal the deformation resistance of asphalt mixtures. The three-point bending test was used to represent the low-temperature performance of the mixtures. The immersion Marshall test was chosen to reflect the water stability, and the SCB test was conducted to check the cracking resistance (at medium temperature) of the mixtures. The SEM test was used to show the distribution of the fibers in the mixture to reveal the physical structure strengthening mechanism of the fibers. The FTIR test was used to analyze the chemical composition of the asphalt extracted from the asphalt mixture samples under different aging degrees to better explain the effect of the aging process on the chemical composition of the asphalt material used in the mixture. The test plan is shown in
Table 6.
3.1. Test Methods for High-Temperature Performance
3.1.1. Wheel Tracking Test
The procedures of the wheel tracking test are in accordance with the
Standard Test Methods of Bitumen and Bituminous Mixtures for Highway Engineering (JTG E20-2011) [
31]. The size of the test sample is 300 × 300 × 50 mm. The test load is 0.7 Mpa and the test temperature is 60 °C during the test. Dynamic stability (
DS) is an index to reveal the high temperature performance of the asphalt mixture. The equation of
DS is shown in Equation (1), where
t1 is 45 min,
t2 is 60 min,
d1 is the rutting depth (mm) at 45 min,
d2 is the rutting depth (mm) at 60 min, N is the rotation speed of the wheel (42 rpm),
C1, C2 are the test coefficients and were set as 1.0 in this test. Three specimens were used to determine
DS.
3.1.2. Uniaxial Penetration Test
The uniaxial penetration test adopted in this paper is specified in the
Specifications for Design of Highway Asphalt Pavement (JTG D50-2017) [
33]. This test is used to reflect the high temperature property of the asphalt mixtures specimen (
Figure 3a) of which the shape is a cylinder (the diameter is 150 mm and the height is 100 mm). The load is applied using a metal column (
Figure 3b) of which the diameter is 42 mm and the height is 50 mm. The test temperature is 60 °C and the loading velocity is 1 mm/min. The equation of penetration stress
σp (MPa) and the uniaxial penetration strength τ
0 (MPa) is listed in Equations (2) and (3).
F (N) is the maximum load,
Ac (mm
2) is the area of the cross section of the metal column and
f is sample dimension correction coefficient and this
f is set as 0.350 in this test. Four specimens were used to determine the uniaxial penetration strength.
3.2. Test Methods for Cracking Resistance
The three-point bending test and the SCB test was conducted to check the cracking resistance at low and medium temperature respectively.
3.2.1. Three-Point Bending Test
The steps of the test are contained in the
Standard Test Methods of Bitumen and Bituminous Mixtures for Highway Engineering (JTG E20-2011) [
31]. The size of the test specimen is 250 × 30 × 35 mm, the test temperature is −10 °C and the loading speed is 50 mm/min. The maximum bending tensile strain when failure is used to describe the low temperature property of the asphalt mixture. The calculation equations of
εB are listed in Equation (4). Where
L, and
h is the span and height of the specimen respectively,
d is the maximum deflection at midspan. Four specimens were used to determine the bending tensile strain.
3.2.2. SCB Test
The SCB test is conducted according to AASHTO TP 124 [
34]. The test temperature is 25 °C. This test is designed according to the Fracture mechanics theory. The cross section of the specimen is semicircle-shaped (the radius is 75 mm), and the specimen is pre-cut for a certain length called pre-cut length (the pre-cut length is 15 mm). The difference between the radius of the specimen and the pre-cut length is called the ductile zone length (DZL).
Gf is the fracture energy and it is calculated according to Equation (5), where
Wf is the integral of the load-displacement curve, and
Arealig is the product of the DZL and the thickness of the specimen (t = 50 mm).
FI index is adopted to reflect the crack propagation rate and it is calculated using Equation (6), where |m| is the absolute value of the slope at the inflection point after the peak of the loading value.
FI value is negatively correlated with the crack propagation rate. Four specimens were used to determine the
FI.
In this paper, fracture toughness (
KIC) is also adopted to evaluate the cracking resistance of mixtures. This index is calculated according to AASHTO TP 105 [
35], shown as Equation (7).
where:
P is the applied load (MN);
r is the specimen radius (m);
t is the specimen thickness (m);
a is the notch length (m);
YI(0.8) is the normalized stress intensity factor, calculated with Equation (8).
3.3. Immersion Marshall Test
The Immersion Marshal test is used to evaluate the water stability of the asphalt mixture. The steps of the test are contained in the
Standard Test Methods of Bitumen and Bituminous Mixtures for Highway Engineering (JTG E20-2011) [
31]. Two sets of four specimens were used to determine the Marshall residual stability
MS0 (%). This index is adopted to represent the water stability of asphalt mixture. The equation of MS
0 is shown in Equation (9), where
MS is the normal Marshall stability and
MS1 is the Marshall stability of the specimen after being immersed into water for 48 h at 60 °C.
3.4. SEM Test
The SEM tests were conducted using the scanning electron microscope produced by Carl Zeiss Microscopy GmbH, Oberkochen, Germany. The test samples were plated by gold using the vacuum coating machine and then been observed by the SEM. SEM images were adopted to analyze the strengthening mechanism of the fibers in the mixtures.
3.5. FTIR Test
The Fourier transform infrared spectrometer (FTIR) adopted in this paper is made by Perkinelmer Instruments Co., Ltd., Shanghai branch, Shanghai, China. The asphalt in the SMA-13 mixtures under different aging degrees was extracted from the mixtures using the vacuum extractor (the medium is trichloroethylene) and tested using the FTIR to find the changing pattern of the chemical functional group in the asphalt to better explain the effect of the aging degree on the chemical composition of the asphalt used in the mixtures.
5. Conclusions and Suggestions
In this paper, the long-term performance of SMA-13 containing different fibers was compared. The following conclusions can be drawn after conducting this research:
- (1)
The high-temperature performance of the BFSMA-13 is better than that of the LFSMA-13 at different aging degrees. The high-temperature performance of BFSMA-13 increases with the increase of the aging degree, while the aging process decreases the high-temperature property of LFSMA-13.
- (2)
The cracking resistance of BFSMA-13 is better than that of LFSMA-13 at different aging stages. The test results proved that BFSMA-13 is more capable of deformation and less prone to cracking at low and medium temperatures.
- (3)
The Marshall stability, immersed Marshall stability, and the residual Marshall stability of BFSMA-13 are greater than that of LFSMA-13, which shows that basalt fiber can better improve the strength and the water stability of SMA-13 mixture than lignin fiber.
- (4)
Different properties of BF and LF lead to their different roles in the mixture. BF can improve the performance of asphalt mixtures by acting in concert with the asphalt mixture. LF can absorb excess free asphalt in SMA-13, and it is not as good as BF in improving the performance of the mixture.
- (5)
At the characteristic peak, the increasing percentage of the peak areas in the spectrum of SBSBF is lower than those in the SBSLF as the mixture ages, indicating that the aging process has a greater impact on the chemical composition of SBSLF than the SBSBF.
Some suggestions are made for further works: (1) the aging method used in this paper only involves thermal aging, and other aging conditions should be adopted, such as ultraviolet light aging; (2) the fatigue properties of asphalt mixtures were not tested in this paper and should be conducted in the future; (3) properties of fiber asphalt mastic at different aging conditions should be tested in further studies; and (4) the reinforcement mechanism of fiber on asphalt mixtures needs to be further clarified.